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Beilstein J. Org. Chem. 2019, 15, 1460–1467, doi:10.3762/bjoc.15.146
Graphical Abstract
Scheme 1: (a) Chemical structures of the reported tetralactam macrocycles with aromatic sidewalls; (b) synthe...
Figure 1: 1H NMR spectra (500 MHz, CDCl3) of a) 1 at 298 K, b) 1 at 223 K, and c) 2 at 298 K.
Figure 2: Two different views of the X-ray single crystal structure of 1 obtained from its CH3CN solution.
Figure 3: Partial 1H NMR spectra (500 MHz, CDCl3, 0.5 mM, 298 K) of 1 and the equimolar mixture with TBA[AuCl4...
Figure 4: ESI mass spectrum of complex AuCl4−@1.
Figure 5: Energy-minimized structure of a) AuCl4−@1 and b) AuCl4−@2 at the level of theory of PM3 by using Sp...
Figure 6: a) Fluorescence emission spectra of 1 (20 µM) upon addition of different amounts of TBA[AuCl4] (con...